The extracts were solvent exchanged into ACN
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micro neddling They were dried with sodium sulfate, concentrated by KD evaporation, and fractionated by gel permeation chromatography (GPC) with DCM. The extracts were solvent exchanged into ACN, followed by ENVI Carb clean up with 48 ml of ACN. Lastly, they were concentrated again to 1 ml and transferred to GC vials. micro neddling
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